I-2-chloro-5-chloromethyl pyridine
Ulwazi Oluyisisekelo:
Igama lekhemikhali: 2-chloro-5-chloromethyl pyridine
Inombolo ye-CAS: 70258-18-3
Ifomula yemolekyuli: C6H5Cl2N
Isisindo se-molecule: 162.02
Inombolo ye-EINECS: 615-091-8
Ifomula yesakhiwo:
Izigaba ezihlobene: Abaphakathi - abaphakathi kwezibulala-zinambuzane; Abaphakathi kwezemithi; Izinto zokusetshenziswa zamakhemikhali ezinto eziphilayo kanye neziphakathi;
Iphuzu elincibilikayo: 37-42 °C(lit.) Iphuzu elibilayo: 267.08°C (isilinganiso esinzima) Ukuminyana: 1.4411 (isilinganiso esinzima) Inkomba ye-Refractive: 1.6000 (isilinganiso) Iphuzu elikhanyayo: >230 °F Ukunyibilika: I-Soluble ku-DMSO (a kancane), i-methanol (encane), engancibiliki emanzini. Umlingiswa: i-beige crystal. I-acidity coefficient (pKa)-0.75±0.10(Kubikezelwe)
| ukucaciswa | iyunithi | ejwayelekile |
| Ukubukeka | Ayinambala ukuya ku-beige crystal | |
| Okuqukethwe okuyinhloko | % | ≥98.0% |
| Umswakama | % | ≤0.5 |
I-2-chloro-5-chloromethyl pyridine (i-CCMP) iyindawo ebalulekile yemithi futhi iyingxenye ebalulekile yokuhlanganiswa kwama-pyridine pesticide agents afana ne-imidacloprid, i-acetamiprid, i-fluazinam, njll.
Ziningi izindlela zokuhlanganisa ze-2-chloro-5-chloromethyl pyridine. Njengamanje, i-2-chloro-5-methylpyridine isetshenziswa njengento eluhlaza embonini, okungukuthi, i-2-chloro-5-methylpyridine i-chlorine nge-2-chloro-5-methylpyridine phambi kwe-catalyst yokuthola i-2-chloro. -5-chloromethyl pyridine. I-2-chloro-5-methylpyridine kanye ne-solvent yengezwe kuketela ye-chlorination, i-catalyst yanezelwa, futhi igesi ye-chlorine yafakwa ekuphenduleni ngaphansi kwesimo se-reflux. Ngemva kokusabela, ingcindezi yokuqala yasemkhathini yahlakazwa, bese ingxenyana yangaphambili yasuswa nge-vacuum ku-kettle ye-distillation, futhi i-2-chloro-5-methylpyridine yatholakala ngaphansi kweketela. Ngaphezu kwe-, kunezinhlobonhlobo zemizila ehlukene esebenzisa i-niacin njengempahla eluhlaza, i-3-methylpyridine njengempahla eluhlaza, i-2-chloro-5-trichloromethyl pyridine njengento eluhlaza. Isici esivamile salezi zindlela ukwakheka kweringi ye-pyridine elandelwa ukuqedwa kwe-chloromethylation. Omunye umzila othuthukiswe yi-United States Rayleigh Company (ReillyIndustriesInc.) uthatha i-cyclopentadiene kanye ne-propanal njengezinto zokuqala zokusetshenziswa ukuze i-cyclosynthesize ngokuqondile i-2-chloro-5-chloromethyl pyridine, futhi ubumsulwa bomkhiqizo buphakeme bufike ku-95%, ngaphandle kwe-isomer 2. -Chloro-3-chloromethyl pyridine.
25Kg/umgqomo; Ukupakisha ngokuvumelana nezidingo zekhasimende.
Lo mkhiqizo kufanele ugcinwe esitsheni esivaliwe futhi ugcinwe endaweni epholile neyomile ngesikhathi sokugcinwa nokuhamba. Ungaxubani nama-oxidants okuthutha nokugcina.
